PREPARATION OF CREAM ROUGE AND DEODORANT

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PREPARATION OF CREAM ROUGE

INTRODUCTION:
       Rouge is a cosmetics used to apply color to the cheeks. Rouge is used to simulate a natural glow and must look subtle. Modern rouge preparations come in the forms of liquid, cream and dry solids forms. Cream or gel rouge has better staying power, while powder rouge comes in larger variety of shades. Creams rouge tend to use humectants or silicones to deliver the colorants while gels, tints and stains are often water based. However, cream rouges are less natural looking and often more difficult to apply. In particular, tints and stains are not very blendable which can result in an “overdone” look. Cream rouges are usually sold in a small pot or stick and are quite thick, while gels, tints and stains are usually in a tube or bottle (almost like a nail polish bottle) and range from medium thickness to the consistency of water. Choice of rouge color depend on our complexion (light, medium, or dark) and secondly on the look that we want to achieve such as fresh or structured, natural or made-up. If you wish to add some freshness and a healthy glow to your face, choose a shade from the cool palette. Any kind of pink is a good choice for lighter complexions, while cool berries and plum shades will work for deeper skin tones. Cream rouges are great for women who have drier skin since the humectants provide a hydrating benefit.
       Rouge or blusher has many functions which can be used separately or together. Firstly, rouge can be used to add shape to the face. It is achieved by applying a matte neutral shade of rouge like beige for example, directly underneath the cheek bone. By applying a thin band of rouge tucked directly under the cheek bone, you will create the illusion of depth directly under the bone and thus creating more shape to the face. Besides, rouge also can be used to soften the cheek bones. Cheek bones that are too obvious (often on very thin people or well- shaped faces), can be made to look less obvious by applying the rouge on top of the cheek bone area. Once you have added shape to your face or softened your cheek bone, you can add natural pink or peach shades to the front of the cheek area and this application adds color to the face. Adding color to the front of the cheek area creates a more healthy appearance on the skin. Rouge also can be used to add glow to the face. 

OBJECTIVES:
  1.  To formulate cream rouge.
  2.  To formulate cream rouge from two commercial hard lipstick preparations.
  3.  To study the factor affecting color shading in cream rouge.
  4.  To evaluate the effect of storage condition on the final product.


APPARATUS:       
Beaker, evaporating dish, spatula, dropper, thermometer, weighing boat, glass rod, filter paper and water bath.

INGREDIENTS:
Cocoa butter, beeswax, cetyl alcohol, wool fat, liquid paraffin, borax, colorant (erythrosine) and water as much as is sufficient

PROCEDURES:

I.            Preparation of cream rouge
  1.  80g of the basic cream formulation was prepared.
  2.  50g of a cream rouge was prepared by using 2% of soluble red coloring agent.
  3.  4 other cream rouge preparations was prepared by diluting the 2% cream rouge accordingly to obtain various shades of color.
  4.  The suggested concentration of coloring agent: 0.125-2%
II.            Effects of storage on the finished products
  1.  The preparation was kept in the dark and also exposed to sunlight for two months.
  2.  Criteria for evaluation of rouge preparation was set up.


FORMULATION:

BASIC POWDER FORMULATION

80g ofC0 (0%)
50g of C2 (2%)
Cocoa butter
5%
4.0g
2.5g
Beeswax
12%
9.6g
6.0g
Cetyl alcohol
1%
0.8g
0.5g
Wool fat
5%
4.0g
2.5g
Liquid paraffin
30%
24.0g
15.0g
Borax
1%
0.8g
0.5g
Colorants (Erythrosine)
2%
xxx
1.0g
Water qs ad
100%
80g
50.0g

Table 1

Code
Colorant (%)
Amount of C2
Amount of C0
Total amount of rouge (g)
C1
2
20
-
20
C2
1
15
10
20
C3
0.5
10
15
20
C4
0.25
5
17.5
20
C5
0.125
2.5
18.75
20

Total (g)
38.75 (~50)
47.5 (~80)


Table 2

RESULT:


                          
Table 3: Cream rouge without light


Table 4: Cream rouge when exposed to sunlight

DISCUSSION:
          In preparation of cream rouge, we need some important ingredients such as cocoa butter, beeswax, cetyl alcohol, wool fat, liquid paraffin, borax, colorant (erythrosine) and water as much as is sufficient. Cocoa butter is oil extracted from cocoa beans, used as an emollient and with properties similar to those of other non-fragrant plant oils. Cocoa butter is a rich source of antioxidant polyphenols; in vitro research has shown it helps improve skin elasticity and promote healthy collagen production (Source: International Journal of Cosmetic Science, October 2008, pages 339–345). It is temporarily protects injured or exposed skin from harmful or annoying stimuli and may provide relief to the skin. Cocoa butter also slows the loss of water from the skin by forming a barrier on the skin's surface. Beeswax and the plant waxes help to keep an emulsion from separating into its oil and liquid components, especially in cosmetics and personal care products that require a creamy consistency. These waxes also increase the thickness of the lipid (oil) portion of solid and stick-like products, giving them structure, allowing for a smooth application, and keeping them solid. Cetyl alcohol is a fatty alcohol that is either produced from the end products of the petroleum industry, or derived from plants (palm oil-palmityl alcohol). It comes in the form of a white, waxy solid. It works as an emollient, emulsifier, thickener and carrying agent for other ingredients contained in rouge formulation. It keeps the oil and water parts of an emulsion from separating, and gives products good spreadability. As a thickening agent and surfactant, it helps alter the viscosity and increase the foaming capacity of non-aqueous and aqueous solutions. Wool fat (lanolin) resembles skin’s own sebum. It is highly emollient and an effective moisturiser. It is cushioning and protects the skin. Lanolin is an excellent moisturising ingredient for dry skin, as it emulsifies water on the skin and holds it there; its cushioning, plumping effect is noticeable. It is a perfect ingredient for barrier creams, baby lotions and eczema creams. It creates a protective film over the skin, allowing it to function and breathe naturally. Liquid paraffin, which is a mineral oil is excellent in forming thin layers with good barrier properties. It works by providing a layer of oil on the surface of the skin to prevent water evaporating from the skin surface. It helps to exfoliate the human skin and make it younger looking. It has a great moisturizing property. A thin layer of mineral oil will slow down the loss of moisture and rehydrate your skin very quickly.  It has also been found to be very helpful as a protective layer for the skin. Borax or sodium borate, a white crystalline mineral generally used as an emulsifier or cleanser. Adding colorant into this formulation creates a more healthy appearance when applying onto the skin. Adding color to the face is very popular, it gives the face an immediate lift and healthy modern look. 
          Firstly, the cocoa butter, beeswax, cetyl alcohol, borax and wool fat were melted in liquid paraffin at about 60 degree Celsius in evaporating dish by using water bath according to the formulation for 80g of C0 (without colorant) cream rouge. After that, purified water, at about 60 degree Celsius was added into the molten mixture and the mixture was stirred gently until cool and smooth cream is formed. Step 1 and 2 were repeated for the preparation of 50g of C2 (with colorants) by adding 1g colorants. Then, 5 cream rouges were prepared according to the exact amount of C0 and C2 based on the table 2.



          Cream rouge can be divided into two phases which are the oil phase and water phase. The usual ingredients of oil phase in cream rouge are cocoa butter, beeswax, wool fat and liquid paraffin. Meanwhile, the water phase is usually the preservatives and colorants. From the chart on the result above, we could know that the concentration of the colorant is the one will determine the colour shadings of the cream rouge.  In this rouge cream preparation, two creams formulation are made up. C0 is the basic formulation of cream without addition of colorant, but for C2 is the formulation  that has been added 2% of colorant of the total weight of the formulation.Then, the cream with the 2% colorants is diluted with the basic cream (C0) with specific proportion to produce 5 rouge creams with different colour shading. The higher the concentration of colorants in the formulation, the darker the colour of the products. Therefore, it can be observed that the colour of the five cream rouges produced are vary from each other and their colour are getting lighter and lighter from C1 to C1.

CONCLUSION:
          As a conclusion, the concentration of colorants will determine the colour that is shown in cream rouge . Higher concentration of colorant will produce darker colour. Storage condition and also the sunlight may cause instability on the rouge products. The steps that could be modified is increase the concentration of colorant since the colour of the cream rouge is too light and does not give a strong colour effect on the skin. Besides, storage condition test should be lengthened to get more accurate results. The stability test  that the rouge is kept in the dark and also exposed to sun lights also give unaccurate result due to amount of sunlight that the rouge exposed to can vary day by day and pollution such as dust particles play a part in variation.The test can be replaced by laboratory controlled tests because they tend to be more reproducible as all conditions are finely controlled.

REFERENCES:
  1. http://www.cosmeticsandskin.com/bcb/rouge.php









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PREPARATION OF DEODORANT

OBJECTIVE:
To prepare a deodorant and evaluate a deodorant’s stability and safety.

INTRODUCTION:
Deodorants and anti-perspirants are preparation that can mask, remove or reduce the unpleasant odor on the body due to sweat. Sweat on its own does not generally have a smell; bacteria present on the surface of the skin digests the sweat and the digestion & breakdown products cause the odor. Therefore, a deodorant functions by decreasing the bacteria population on the skin or by adding fragrance to the body to overcome the foul odor. On the other hand, an anti-perspirant functions by reducing the production of sweat through its astringent property.

APPARATUS:
Water bath, evaporating dish, glass rod, weighing boat, dropper, beaker

INGREDIENTS:
Beeswax, cocoa butter, coconut oil , silicone oil, vitamin E oil, corn starch, essential oil/ perfumes

PROCEDURE:

Ingredients
Percentage (%)
Weight (g) (for 20g of product)
Beeswax
20
4
Cocoa butter
30
6
Coconut oil
30
6
Silicone oil
3
0.6
Vitamin E oil
2
0.4
Corn starch
12
2.4
Essential oil/ Perfumes
Not more than 3
Less than 0.6

A. PRODUCTION
  1. All the ingredients are weighed according to the table above.
  2. Beeswax and the cocoa butter are heated until just melted. Then, the coconut, silicone and vitamin E oils are added.
  3. The essential oils or perfumes are added when all the oils and fats have melted.
  4. The mixture is mixed in the corn starch until homogenous by using hand mixer.
  5. The molten mixture is poured into a container and it is allowed to cool until hardens.
  6. Steps 1 to 5 are repeated by using different types of essential oils or perfumes.


B. EVALUATION OF PRODUCTS
  1. The product is tested by each member of the group.
  2. A simple questionnaire that allows each person to compare the effectiveness of each product and whether the fragrance incorporated is irritating to the skin is devised.
  3. The product is tested after taking a shower in the morning and when the body is dried. One side of underarm functions as a control while the product is applied on the opposite underarm.
  4. Not more than 1g of product is applied on the underarm by using the application provided.
  5. After exactly 9 hours of normal activities, the questionnaire is filled in. The questionnaire is shown as table below.
Questionnaire

Questions
1
2
3
4
5
How do you think about the appearance of the product?





How do you feel after applying the product?





Does the fragrance still remain?





Does it significant in masking odor?






Tips: 1 – Worst, 2 – Bad, 3 – Normal, 4 – Great, 5 – Excellent

Does the deodorant produce unpleasant smell after applied? (Yes / No)

RESULTS:

Questions
1
2
3
4
5
How do you think about the appearance of the product?
-
-
3
2
-
How do you feel after applying the product?
-
-
1
4
-
Does the fragrance still remain?
1
2
2
-
-
Does it significant in masking odor?
-
2
3
-
-

Based on the result obtained from group members, the appearance of the product is just normal and maybe a little bit not so attractive. Secondly, most 4 of group members think that they feel great after apply the product, without feeling any greasy. But, the odor masking of the product is not that significant and the fragrance does not remain for a long time.

DISCUSSION:

          Through this experiment, we learnt the correct ways to produce a deodorant. As we know that the use of deodorants is to mask, remove or reduce the unpleasant body odor that causes by the metabolic products of bacteria in some parts of the body. Thus, by reducing the number of bacteria at particular body parts or blocking the sweat pores to avoid sweating, deodorants can significantly reduce the unpleasant smell of the body.
         Although deodorants are good in masking, reducing or removing the body odor, some deodorants may causes irritation due to some of the ingredients such as certain kinds of essential oils and fragrances. Hence, the content of the deodorants must be well controlled and be tested before we can actually market them. Sometimes, the ingredients may also cause unwanted blocking of sweating gland and causes some skin problems as the sweat cannot be expelled through sweat glands.
Besides, the feeling of consumers after applying the product is important too. The product should not be too greasy as it will causes unpleasant feeling to consumers. Moreover, the product should not easily evaporate too. This is because, if the product evaporates in a quick manner, the fragrance will disappear soon and causes insignificant masking of body odor. Finally, the picking of the fragrances and essential oils for the product is very important too. This is due to some fragrances when mixed with body sweat; it will produce an even worst smell instead of masking the unpleasant smell of the body. This will definitely causes the product become useless to consumers.
               Thus, a good deodorant must be able to mask, reduce or remove the bad smell of the body and do not causes any unwanted effect such as irritation, blocking of sweat glands and blackening of skin to the consumer.

CONCLUSION:
The deodorants can be made by using fusion method of beeswax, cocoa butter, coconut oil, silicone oil, vitamin E oil, corn starch and little volume of essential oil or perfumes.

REFERENCES: 

  1. Cosmetics Q&A: "Personal Care Products". U.S. Food and Drug Administration.
  2. Antiperspirant Drug Products For Over-the-Counter Human Use; Final Monograph". U.S. Food and Drug Administration.  
  3. Laden, Karl (1999). Anti-Perspirants and Deodorants, Second Edition. CRC Press. ISBN 978-0-8247-1746-9.


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